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Inorganic & Coordination Chemistry

Van Arkel Process

A purification method in which a metal is converted to a volatile iodide and then decomposed on a hot filament.

Formula / equation Ti + 2I₂ ⇌ TiI₄
Unit °C

In depth

The impure metal reacts with iodine at moderate temperature to form a volatile iodide that leaves the non-volatile impurities behind. The vapour then decomposes on a filament heated above 1400 °C, depositing ultrapure metal and releasing the iodine for reuse.

Examples in the real world

Producing ultrapure titanium and zirconium for nuclear and aerospace applications.